An easy and efficient method for the synthesis of hydroximoyl chloride from nitro olefin and silyl enol ether

Ming Chung Yan, Zhijay Tu, Chunchi Lin, Ching Fa Yao*

*此作品的通信作者

研究成果: 雜誌貢獻期刊論文同行評審

5 引文 斯高帕斯(Scopus)

摘要

Reactions of nitro olefin 1 with silyl enol ether 2 in the presence of TiCl4 in CH2Cl2 at 0°C gave high yields of hydroximoyl chloride 3. When the hydroximoyl chloride 3 was treated with Et3N in the presence of dipolarophile, the corresponding 2-isoxazolines were obtained.

原文英語
頁(從 - 到)7991-7994
頁數4
期刊Tetrahedron Letters
43
發行號44
DOIs
出版狀態已發佈 - 2002 十月 28

ASJC Scopus subject areas

  • 生物化學
  • 藥物發現
  • 有機化學

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