Quantification of anthocyanosides in grapes by QuEChERS and biphenyl-UHPLC tandem mass spectrometry

Lun Chi Yang; Sung Fang Chen

doi:10.38212/2224-6614.3427

Quantification of anthocyanosides in grapes by QuEChERS and biphenyl-UHPLC tandem mass spectrometry

Lun Chi Yang, Sung Fang Chen^*

^*Corresponding author for this work

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

In this study, the QuEChERS and UHPLC-MS/MS method using a biphenyl stationary phase was developed and applied for the rapid separation of 12 anthocyanosides in grapes. Efficient separation was achieved for a wide range of mono-and un-glycosylated anthocyanosides. The linear ranges of the target anthocyanosides were 0.5e500 ng mL^-1. The intra-and inter-day precisions were both below 11.8%. Anthocyanosides in grapes from different sources were suc-cessfully quantified. Thus, the developed QuEChERS and UHPLC-MS/MS method provide an attractive alternative for the quantification of anthocyanosides in grapes.

Original language	English
Article number	5
Pages (from-to)	382-401
Number of pages	20
Journal	Journal of Food and Drug Analysis
Volume	30
Issue number	3
DOIs	https://doi.org/10.38212/2224-6614.3427
Publication status	Published - 2022

Keywords

Anthocyanosides
Biphenyl stationary phase
LC-MS/MS
QuEChERS
Quantification

ASJC Scopus subject areas

Food Science
Pharmacology

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10.38212/2224-6614.3427

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title = "Quantification of anthocyanosides in grapes by QuEChERS and biphenyl-UHPLC tandem mass spectrometry",

abstract = "In this study, the QuEChERS and UHPLC-MS/MS method using a biphenyl stationary phase was developed and applied for the rapid separation of 12 anthocyanosides in grapes. Efficient separation was achieved for a wide range of mono-and un-glycosylated anthocyanosides. The linear ranges of the target anthocyanosides were 0.5e500 ng mL-1. The intra-and inter-day precisions were both below 11.8%. Anthocyanosides in grapes from different sources were suc-cessfully quantified. Thus, the developed QuEChERS and UHPLC-MS/MS method provide an attractive alternative for the quantification of anthocyanosides in grapes.",

keywords = "Anthocyanosides, Biphenyl stationary phase, LC-MS/MS, QuEChERS, Quantification",

author = "Yang, {Lun Chi} and Chen, {Sung Fang}",

note = "Publisher Copyright: {\textcopyright} 2022 Taiwan Food and Drug Administration.",

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T1 - Quantification of anthocyanosides in grapes by QuEChERS and biphenyl-UHPLC tandem mass spectrometry

AU - Yang, Lun Chi

AU - Chen, Sung Fang

PY - 2022

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N2 - In this study, the QuEChERS and UHPLC-MS/MS method using a biphenyl stationary phase was developed and applied for the rapid separation of 12 anthocyanosides in grapes. Efficient separation was achieved for a wide range of mono-and un-glycosylated anthocyanosides. The linear ranges of the target anthocyanosides were 0.5e500 ng mL-1. The intra-and inter-day precisions were both below 11.8%. Anthocyanosides in grapes from different sources were suc-cessfully quantified. Thus, the developed QuEChERS and UHPLC-MS/MS method provide an attractive alternative for the quantification of anthocyanosides in grapes.

AB - In this study, the QuEChERS and UHPLC-MS/MS method using a biphenyl stationary phase was developed and applied for the rapid separation of 12 anthocyanosides in grapes. Efficient separation was achieved for a wide range of mono-and un-glycosylated anthocyanosides. The linear ranges of the target anthocyanosides were 0.5e500 ng mL-1. The intra-and inter-day precisions were both below 11.8%. Anthocyanosides in grapes from different sources were suc-cessfully quantified. Thus, the developed QuEChERS and UHPLC-MS/MS method provide an attractive alternative for the quantification of anthocyanosides in grapes.

KW - Anthocyanosides

KW - Biphenyl stationary phase

KW - LC-MS/MS

KW - QuEChERS

KW - Quantification

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Quantification of anthocyanosides in grapes by QuEChERS and biphenyl-UHPLC tandem mass spectrometry

Abstract

Keywords

ASJC Scopus subject areas

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