Interfacing ASE and HPLC for the determination of PAH in soil

Chien Wen Chen; Yun Yuan Wang; Gaston J.C. Wu

doi:10.1002/jccs.199900039

Interfacing ASE and HPLC for the determination of PAH in soil

Chien Wen Chen^*, Yun Yuan Wang, Gaston J.C. Wu

^*Corresponding author for this work

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

Abstract

A method was developed to couple an accelerated solvent extraction system (ASE) with high performance liquid chromatography (HPLC) for the analysis of PAH in soil samples. The resolution of HPLC is well maintained while the advantages of ASE, fast extraction, less solvent consumption and ease of operation, are well expressed. The precision and accuracy of this method are verified by a series of analyses of reference material, and the precision of retention from multiple injection indicates minimum loss of chromatographic resolution by the interface of this technique. Detection limits for the studied PAH range from 0.07 ng/Kg to 0.21 ng/Kg with a fluorescence detector.

Original language	English
Pages (from-to)	245-251
Number of pages	7
Journal	Journal of the Chinese Chemical Society
Volume	46
Issue number	2
DOIs	https://doi.org/10.1002/jccs.199900039
Publication status	Published - 1999

Keywords

Accelerated solvent extraction (ASE)
High performance liquid chromatography (HPLC)
Polycyclic aromatic hydrocarbons (PAH)
Soil

ASJC Scopus subject areas

General Chemistry

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10.1002/jccs.199900039

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abstract = "A method was developed to couple an accelerated solvent extraction system (ASE) with high performance liquid chromatography (HPLC) for the analysis of PAH in soil samples. The resolution of HPLC is well maintained while the advantages of ASE, fast extraction, less solvent consumption and ease of operation, are well expressed. The precision and accuracy of this method are verified by a series of analyses of reference material, and the precision of retention from multiple injection indicates minimum loss of chromatographic resolution by the interface of this technique. Detection limits for the studied PAH range from 0.07 ng/Kg to 0.21 ng/Kg with a fluorescence detector.",

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AU - Chen, Chien Wen

AU - Wang, Yun Yuan

AU - Wu, Gaston J.C.

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N2 - A method was developed to couple an accelerated solvent extraction system (ASE) with high performance liquid chromatography (HPLC) for the analysis of PAH in soil samples. The resolution of HPLC is well maintained while the advantages of ASE, fast extraction, less solvent consumption and ease of operation, are well expressed. The precision and accuracy of this method are verified by a series of analyses of reference material, and the precision of retention from multiple injection indicates minimum loss of chromatographic resolution by the interface of this technique. Detection limits for the studied PAH range from 0.07 ng/Kg to 0.21 ng/Kg with a fluorescence detector.

AB - A method was developed to couple an accelerated solvent extraction system (ASE) with high performance liquid chromatography (HPLC) for the analysis of PAH in soil samples. The resolution of HPLC is well maintained while the advantages of ASE, fast extraction, less solvent consumption and ease of operation, are well expressed. The precision and accuracy of this method are verified by a series of analyses of reference material, and the precision of retention from multiple injection indicates minimum loss of chromatographic resolution by the interface of this technique. Detection limits for the studied PAH range from 0.07 ng/Kg to 0.21 ng/Kg with a fluorescence detector.

KW - Accelerated solvent extraction (ASE)

KW - High performance liquid chromatography (HPLC)

KW - Polycyclic aromatic hydrocarbons (PAH)

KW - Soil

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Interfacing ASE and HPLC for the determination of PAH in soil

Abstract

Keywords

ASJC Scopus subject areas

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