Interfacing ASE and HPLC for the determination of PAH in soil

Chien Wen Chen, Yun Yuan Wang, Gaston J. C. Wu

Research output: Contribution to journalArticle

5 Citations (Scopus)

Abstract

A method was developed to couple an accelerated solvent extraction system (ASE) with high performance liquid chromatography (HPLC) for the analysis of PAH in soil samples. The resolution of HPLC is well maintained while the advantages of ASE, fast extraction, less solvent consumption and ease of operation, are well expressed. The precision and accuracy of this method are verified by a series of analyses of reference material, and the precision of retention from multiple injection indicates minimum loss of chromatographic resolution by the interface of this technique. Detection limits for the studied PAH range from 0.07 ng/Kg to 0.21 ng/Kg with a fluorescence detector.

Original languageEnglish
Pages (from-to)245-251
Number of pages7
JournalJournal of the Chinese Chemical Society
Volume46
Issue number2
DOIs
Publication statusPublished - 1999 Jan 1

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Keywords

  • Accelerated solvent extraction (ASE)
  • High performance liquid chromatography (HPLC)
  • Polycyclic aromatic hydrocarbons (PAH)
  • Soil

ASJC Scopus subject areas

  • Chemistry(all)

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