Addition of functionalized zinc‐copper reagents to the title complexes proceeds in a highly diastereoselective fashion to afford dienol complexes. The relative configurations of adducts 3d were determined by single X‐ray diffraction analysis.
- (Diene‐aldehyde)Fe(CO) complex
- Diastereomeric ratio
- Diastereoselective alkylation
- Functionalized zinc‐copper reagents
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